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6R/S-deutero-a-d-mannopyranoside 1-phosphate

Miller, Gavin; Ahmadipour, Sanaz


Sanaz Ahmadipour


6R/S-deutero-a-d-mannopyranoside 1-phosphate was synthesised from a C6 aldehydic mannose thioglycoside donor in four steps. Using NaBD4 as the reductant, isotopic enrichment at C6 was achieved and the resultant C6-deuterated material was converted through to the glycosyl 1-phosphate using a protection/glycosylation/deprotection sequence. The product was fully characterised by 1H, 13C, 31P and 2D NMR, alongside MS analysis.

Journal Article Type Article
Acceptance Date Jun 24, 2019
Publication Date Jun 27, 2019
Journal Molbank
Publisher MDPI
Peer Reviewed Peer Reviewed
Volume 2019
Issue 3
Article Number M1068
Keywords mannose; glycosyl-phosphate; deuterium; isotope; NMR
Publisher URL